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Direct structure elucidation by powder X-ray diffraction of a metal-organic framework material prepared by solvent-free grinding

Fujii, Kotaro, Garay, Ana Lazuen, Hill, Janeen, Sbircea, Elena, Pan, Zhigang, Xu, Mingcan, Apperley, David C., James, Stuart L. and Harris, Kenneth David Maclean 2010. Direct structure elucidation by powder X-ray diffraction of a metal-organic framework material prepared by solvent-free grinding. Chemical Communications- Royal Society of Chemistry 46 (40) , pp. 7572-7574. 10.1039/C0CC02635B

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Abstract

Powder X-ray diffraction (XRD) has been exploited to establish the structural properties of a porous interpenetrated mixed-ligand metal–organic framework material prepared by solid-state grinding, recognizing that product phases from mechanochemical synthesis are typically microcrystalline powders. The importance of subjecting the powder XRD data to rigorous scrutiny in such applications is emphasized.

Item Type: Article
Status: Published
Schools: Advanced Research Computing @ Cardiff (ARCCA)
Chemistry
Subjects: Q Science > QD Chemistry
Publisher: Royal Society of Chemistry
ISSN: 1359-7345
Last Modified: 04 Jun 2017 02:51
URI: http://orca.cf.ac.uk/id/eprint/12825

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