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A mechanochemical zinc-mediated barbier-type allylation reaction under ball-milling conditions

Yin, JieXiang, Stark, Roderick T., Fallis, Ian A. and Browne, Duncan L. 2020. A mechanochemical zinc-mediated barbier-type allylation reaction under ball-milling conditions. Journal of Organic Chemistry 10.1021/acs.joc.9b02876
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Abstract

A ball-milling-enabled zinc-mediated Barbier-type allylation reaction is reported. Notably, running the reaction in this manner renders it effective irrespective of the initial morphology of the zinc metal. The process is operationally simple, does not require inert atmospheres or dry solvents, and is reported over a range of aldehyde and ketone substrates; a gram-scale process is demonstrated.

Item Type: Article
Date Type: Published Online
Status: In Press
Schools: Chemistry
Publisher: American Chemical Society
ISSN: 0022-3263
Funders: KESS
Date of First Compliant Deposit: 13 January 2020
Date of Acceptance: 20 December 2019
Last Modified: 14 Jan 2020 11:45
URI: http://orca.cf.ac.uk/id/eprint/128463

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