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Preparation of inner-side tubular zeolite NaA membranes in a continuous flow system

Pera-Titus, Marc, Bausach, Marta, Llorens, Joan and Cunill, Fidel 2008. Preparation of inner-side tubular zeolite NaA membranes in a continuous flow system. Separation and Purification Technology 59 (2) , pp. 141-150. 10.1016/j.seppur.2007.05.038

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Abstract

Zeolite NaA membranes were synthesized on the inner side of porous titania (rutile) asymmetric tubular supports in a flow system where the synthesis gel was circulated through the support with flow rates in the range 1.5–4 mL min−1 by the action of gravity. The syntheses were carried out hydrothermally at 358 K for 6–7 h either with or without previous brush-seeding of the supports. The membranes (10–20 μm in thickness) showed great ability to dehydrate ethanol/water mixtures (92:8, w/w) by pervaporation with selectivities and fluxes, respectively, up to 8500 and 1.2 kg m−2 h−1 at 323 K. The role of intercrystalline defects in the pervaporation performance of the synthesized membranes was also investigated.

Item Type: Article
Date Type: Publication
Status: Published
Schools: Chemistry
Cardiff Catalysis Institute (CCI)
Publisher: Elsevier
ISSN: 1383-5866
Date of Acceptance: 31 May 2007
Last Modified: 13 Oct 2020 11:00
URI: https://orca.cardiff.ac.uk/id/eprint/135396

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