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Chemistry of the phenoxathiins and isosterically related heterocycles. 22. 6,7,9-trimethyl-4-azaphenoxathiin: First reported synthesis of an analog of the 4-azaphenoxathiin ring system

Puig-Torres, Salvador, Martin, Gary E., Smith, Keith, Cacioli, Paul and Reiss, James A. 1982. Chemistry of the phenoxathiins and isosterically related heterocycles. 22. 6,7,9-trimethyl-4-azaphenoxathiin: First reported synthesis of an analog of the 4-azaphenoxathiin ring system. Journal of Heterocyclic chemistry 19 (4) , pp. 879-882. 10.1002/jhet.5570190433

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Abstract

The reaction of 2-chloro-3-thiocyanatopyridine with a substituted spiroepoxycyclohexadienone, which served as a masked phenol with reversed polarity, led to the first reported synthesis of an analog of the 4-azaphenoxathiin ring system. Confirmation of the structure was obtained from the assignment of the 13C-nmr spectrum.

Item Type: Article
Status: Published
Schools: Chemistry
Subjects: Q Science > QD Chemistry
Publisher: Wiley
ISSN: 0022-152x
Last Modified: 04 Jun 2017 02:57
URI: http://orca.cf.ac.uk/id/eprint/14522

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