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Preparation of oxonanes and azonanes by oxidative ring expansion: synthesis of obtusan

Brown, David S., Elliott, Mark Christopher, Moody, Christopher J. and Mowlem, Timothy J. 1995. Preparation of oxonanes and azonanes by oxidative ring expansion: synthesis of obtusan. Journal of the Chemical Society, Perkin Transactions 1 1995 (9) , pp. 1137-1144. 10.1039/p19950001137

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Abstract

Oxonanes can be readily prepared from phthalans by a 3-step procedure involving Birch reduction, selective hydrogenation and oxidation. 2-Ethyl-9-pentyloxonane-3,8-dione has been deoxygenated to give obtusan. The method has been applied to the synthesis of an azonane.

Item Type: Article
Date Type: Publication
Status: Published
Schools: Chemistry
Subjects: Q Science > QD Chemistry
Publisher: RSC Publishing
ISSN: 0300-922X
Last Modified: 04 Jun 2017 04:29
URI: http://orca.cf.ac.uk/id/eprint/39952

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