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Preparation of 9-Membered Cyclic Ethers from Phthalans. Synthesis of Obtusan

Elliott, Mark Christopher, Moody, Christopher J. and Mowlem, Timothy J. 1993. Preparation of 9-Membered Cyclic Ethers from Phthalans. Synthesis of Obtusan. Synlett 1993 (12) , pp. 909-910. 10.1055/s-1993-22648

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Abstract

Phthalans 1-3 have been converted into oxonane-3,8-diones 7-9 by a 3-step sequence involving Birch reduction, hydrogenation and oxidative cleavage; the 2-ethyl-9-pentyl derivative 9 has been deoxygenated to give obtusan 12. The method was extended to the preparation of azonane 15 from isoindoline.

Item Type: Article
Date Type: Publication
Status: Published
Schools: Chemistry
Subjects: Q Science > QD Chemistry
Publisher: Georg Thieme Verlag
ISSN: 0936-5214
Last Modified: 04 Jun 2017 04:29
URI: http://orca.cf.ac.uk/id/eprint/39960

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