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A rapid and efficient protocol for the synthesis of novel nitrothiazolo[3,2-c]pyrimidines via microwave-mediated Mannich cyclisation

Yıldırım, Muhammet, Çelikel, Derya, Dürüst, Yaşar, Knight, David William and Kariuki, Benson 2014. A rapid and efficient protocol for the synthesis of novel nitrothiazolo[3,2-c]pyrimidines via microwave-mediated Mannich cyclisation. Tetrahedron 70 (12) , pp. 2122-2128. 10.1016/j.tet.2014.02.003

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Abstract

Several 6-substituted-8-nitrothiazolo[3,2-c]pyrimidine derivatives have been obtained very efficiently by a multicomponent cyclisation of 2-(nitromethylene)thiazolidine, formaldehyde and various aliphatic or aromatic amines in water, using both microwave irradiation and conventional heating. Reaction yields were considerably higher and the reaction times very much reduced using microwave heating when compared to conventional heating, resulting in the definition of a rapid and efficient synthetic protocol.

Item Type: Article
Date Type: Publication
Status: Published
Schools: Chemistry
Subjects: Q Science > QD Chemistry
Publisher: Elsevier
ISSN: 0040-4020
Last Modified: 04 Jun 2017 06:53
URI: http://orca.cf.ac.uk/id/eprint/66118

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Cited 4 times in Web of Science. View in Web of Science.

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