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New in situ solid-state NMR strategies for exploring materials formation and adsorption processes: prospects in heterogenous catalysis

Harris, Kenneth David Maclean ORCID: https://orcid.org/0000-0001-7855-8598 2016. New in situ solid-state NMR strategies for exploring materials formation and adsorption processes: prospects in heterogenous catalysis. Applied Petrochemical Research 6 (3) , pp. 295-306. 10.1007/s13203-016-0152-3

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Abstract

Solid-state NMR spectroscopy is a powerful technique for studying structural and dynamic properties of solids and has considerable potential to be exploited for in situ studies of chemical processes. However, adapting solid-state NMR techniques and instrumentation for in situ applications are often associated with technical challenges, and for this reason, the opportunities remain underexploited. This paper highlights two experimental strategies that we have developed in recent years for in situ solid-state NMR investigations of solid-state processes. One technique is focused on probing details of the time evolution of materials formation processes, and the other technique is focused on understanding the time evolution of adsorption processes in microporous and mesoporous solid host materials. Each of these in situ solid-state NMR techniques has significant prospects for applications in areas relating to heterogeneous catalysis.

Item Type: Article
Date Type: Publication
Status: Published
Schools: Chemistry
Subjects: Q Science > QD Chemistry
Publisher: Springer
ISSN: 2190-5525
Date of First Compliant Deposit: 23 May 2016
Date of Acceptance: 21 April 2016
Last Modified: 04 May 2023 08:21
URI: https://orca.cardiff.ac.uk/id/eprint/91139

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