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Tetrahydrofuranylation of alcohols using hypervalent iodine reagents

French, Andrew N., Cole, Jonathan and Wirth, Thomas ORCID: https://orcid.org/0000-0002-8990-0667 2004. Tetrahydrofuranylation of alcohols using hypervalent iodine reagents. Synlett (13) , pp. 2291-2294. 10.1055/s-2004-832810

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Abstract

Alcohols are converted to their corresponding 2-tetrahydrofuranyl ethers using (diacetoxyiodo)benzene in THF. Reactions are carried out under reflux, or, more effectively, under microwave irradiation. Yields up to 81% are reported without the use of chlorinated solvents.

Item Type: Article
Date Type: Publication
Status: Published
Schools: Chemistry
Subjects: Q Science > QD Chemistry
Uncontrolled Keywords: hypervalent iodine - bis-THF-ether adduct - oxidations - protecting groups - microwave
Publisher: Georg Thieme Verlag
ISSN: 0936-5214
Last Modified: 18 Oct 2022 12:25
URI: https://orca.cardiff.ac.uk/id/eprint/9766

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